생약 중 잔류 생약의 분석법: GC/MS 에 의한 27종 잔류 규제 농약의 분석

• 영문명: Analysis of Residual Pesticides in Herbal Drugs: GC/MS Analysis of 27 Controlled Pesticides
• 발행기관: 대한약학회
• 저자명: 박만기(Man Ki Park) 박정일(Jeong Hill Park) 윤혜란(Hye Ran Yoon) 윤인병(In Byoung Yoon) 조술연(Sool Yeon Cho) 황귀서(Gwi Seo Hwang)
• 간행물 정보: 『약학회지』제40권 제2호 (1996년), 141~148쪽, 전체 8쪽
• 주제분류: 의약학 > 기타의약학
• 파일형태: PDF
• 발행일자: 1996.04.30

영문 초록

GC/MS analysis of 27 controlled pesticides in herbal drugs was studied. Selected ion monitoring(sim) technique was applied to increase the GC/MS sensitivity. Typical peaks in the mass spectrum of each pesticides were selected as quantitation, comfirmation or alternate ion. Twenty seven pesticides were divided into five groups according to their retention time and the peaks for SIM were programmed accordingly. The combination of two ionization methods, electron impact(EI)-SIM-MS and negative ion chemical ionization(NCI)-SIM-MS, were well-fitted for the detection, confirmation and quantitation of multiclass residual pesticides in herbal drugs.

키워드

Pesticide analysis herbal drug GC/MS SIM CI.