흑연로 원자 흡광 광도법과 유도 결합 플라즈마 질량 분석법을 이용한 혈중 납 농도 비교

• 영문명: Comparison of Blood Lead Concentration Using Graphite Furnace Atomic Absorption Spectrometry (GF-AAs) and Inductively Coupled Plasma-mass Spectrometry (ICP-MS)
• 발행기관: 한국환경보건학회
• 저자명: 강민경(Min-Kyung Kang) 권정연(Jung-Yeon Kwon) 김병권(Byoung-Gwon Kim) 임현주(Hyoun-Ju Lim) 서정욱(Jeong-Wook Seo) 김유미(Yu-Mi Kim) 홍영습(Young-Seoub Hong)
• 간행물 정보: 『1. 한국환경보건학회지』제45권 제3호, 258~266쪽, 전체 9쪽
• 주제분류: 공학 > 환경공학
• 파일형태: PDF
• 발행일자: 2019.06.30

영문 초록

Objectives: In this study, blood lead was analyzed using graphite furnace atomic absorption spectrometry (GFAAs) and inductively coupled plasma mass spectrometry (ICP-MS). We tried to examine the difference and consistency of the analytical values and the applicability of the analytical method. Methods: We selected 57 people who agreed to participate in this study. After confirming the linearity of the calibration standard curves in GF-AAs and ICP-MS, the concentrations of lead in quality control material and samples were measured, and the degree of agreement was compared. Results: The detection limit of the ICP-MS was lower than that of GF-AAs. The coefficient of variation of reference materials was shown to be stable in the ICP-MS and GF-AAs. When the correspondence between the two equipments was verified by bias of the analysis values, a concordance was shown, and approximately 98% of the ideal reference lines were present within ±40% of the deflection. Conclusion: GF-AAs showed high sensitivity to single heavy metal analysis, but it took much time and showed higher detection limit than ICP-MS. Therefore, it would be considered necessary to switch to ICP-MS analysis method, considering that the level of lead exposure is gradually decreasing.

목차

I. 서 론

II. 대상 및 방법

III. 결 과

IV. 고 찰

V. 결 론

키워드

Lead ICP-MS GF-AAs degree of agreement